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Analytical Chemistry Experiment
第8次开课
开课时间: 2025年03月05日 ~ 2025年06月30日
学时安排: 3-5小时每周
当前开课已结束 已有 6 人参加
老师已关闭该学期,无法查看
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spContent=Analytical chemistry experiment is unique in the construction of digital resources. It meets your personalized learning needs. Mobile virtual laboratory helps you simulate the whole process, experience the real experimental scene, and help you become an experimental expert!
Analytical chemistry experiment is unique in the construction of digital resources. It meets your personalized learning needs. Mobile virtual laboratory helps you simulate the whole process, experience the real experimental scene, and help you become an experimental expert!
—— 课程团队
课程概述


The experiment center of chemistry of Dalian University of Technology was elected as the first batch of national experimental teaching demonstration center and the first batch of national virtual simulation experiment teaching center by the Ministry of education. Analytical chemistry experiment is an important basic course of experiment center of chemistry, which is also a basic experiment course of chemistry, chemical engineering, environment, life and other related majors. The teaching contents of the course include guiding class of analytical chemistry experiment, basic operation of instrument, acid-base titration experiment, coordination titration experiment, oxidation-reduction titration experiment, precipitation titration experiment, gas chromatography experiment, liquid chromatography experiment, spectrophotometry experiment and potential analysis experiment. The total class hours of the course are 72. This course can deepen the learners' understanding for various analysis methods, and cultivate their solid basic operation skills. It can also help learners develop a rigorous and practical experimental attitude, a good scientific style and experimental literacy. It can reverse the phenomenon of "grasping medicine according to the prescription" and lack of innovative thinking in the experimental process, and cultivate the learners' innovative practice ability.

Features of this course:

1. Multi form excellent learning resources

 It covers multi integrated and multi-modal learning resources such as micro video, animation, courseware and test questions, so as to realize the guidance of pre-class content.

2. Mobile virtual experiment

 It can simulate the whole process of experiment operation anytime and anywhere, and give the scientific experimental data dynamically. You may really feel the experimental scene.

3. Multi-dimensional electronic experiment report

 It can record the experiment phenomena and data information stereoscopically, and keep the experiment process to the maximum extent.

4. Real time assessment and evaluation system

It can evaluate the whole process of experiment operation in real time, to achieve the quantification and informationization of experimental achievement, and comprehensively improve the degree of curriculum challenges.

This course can realize online teaching in the whole process: to learn the video or other excellent learning resources; to do the preview test; to simulate the operation with virtual experiment; to process the electronic experiment report; to finish the final test. It can meet the personalized learning needs of learners and realize the sharing of high-quality resources.

授课目标

1. To deepen the understanding of various analytical methods and theories. To guide the experimental operation with the theoretical knowledge learned. To improve the ability to analyze and solve practical problems. To lay a solid foundation for independent scientific research in the future.

2. To master the basic knowledge, basic operation skills, typical analysis methods and experimental data processing methods of analytical chemistry experiment.

3. To enhance the understanding of the concept of "quantity". To possess the ability to analyze the experimental data. To learn how to choose experimental methods, conditions and instruments reasonably to ensure the reliability of the experimental results.

4. To cultivate the rigorous work style and realistic work attitude of learners.

 

课程大纲

Charper1 Course Introduction

1.1 Course Guidance

1.2 Laboratory Safety Knowledge

1.3 Online Virtual Experiment

Laboratory Safety Test

Charper2 Basic Operation

2.1 Use of Electronic Analytical Balance

2.2 Use of Buret

2.3 Use of Volumetric Flask

2.4 Use of Pipet

2.5 Use of pH Meter

2.6 Use of UV-Vis Spectrophotometer

2.7 Use of Gas Chromatograph

2.8 Use of Liquid Chromatograph

2.9 Use of Cuvet

2.10 Use of Microliter Pipet

Test of Basic Operation

Charper3 Acid-Base Titration Experiment

3.1 Weighing Practice of Analytical Balances

3.2 Practice of Titration Operation

3.3 Principles of Determination of the Total Alkalinity in Industrial Soda

3.4 Experiment of Determination of Total Alkalinity in Industrial Soda

3.5 Online Virtual Experiment of the Total Alkalinity Determination

Test of Acid-Base Titration Experiment

Charpter4 Coordination Titration Experiment

4.1 Principles of Determination of the Water Hardness

4.2 Experiment of Determination of the Water Hardness

4.3 Online Virtual Experiment of the Determination of the Water Hardness

Test of Coordination Titration Experiment

Charpter5 Redox Titration Experiment

5.1 Principles of Determination of Calcium Content in Calcium Salt

5.2 Experiment of Determination of Calcium Content in Calcium Salt

5.3 Online Virtual Experiment of Determination of Calcium Content in Calcium Salts

Test of Redox Titration Experiment

Charpter6 Experiment of Spectrophotometry

6.1 Principles of Spectrophotometric Determination of Iron with 1,10-Phenanthroline

6.2 Preparation of Standard Solution of Iron(Ⅱ)-phenanthroline Complex

6.3 Use of Cuvet

6.4 Experimental Demonstration of Spectrophotometric Determination of Iron with 1,10-Phenanthroline-1

6.5 Experimental Demonstration of Spectrophotometric Determination of Iron with 1,10-Phenanthroline-2

6.6 Experimental Demonstration of Spectrophotometric Determination of Iron with 1,10-Phenanthroline-3

6.7 Online Virtual Experiment of Spectrophotometric Determination of Iron with 1,10-Phenanthroline

Test of Spectrophotometry Experiment

Charpter 7 Potential Analysis Experiment

7.1 Principles of Determination of Fluoride in Drinking Water by Ion Selective Electrode

7.2 Experiment of Determination of Fluoride in Drinking Water by Ion Selective Electrode

7.3 Online Virtual Experiment of Determination of Fluoride in Drinking Water by Ion Selective Electrode

Test of Fluoride Determination

Charpter8 Gas Chromatography Experiment

8.1 Principles of Analysis of Alcohols by Gas Chromatography

8.2 Use of Microinjector

8.3 Preparation of Standard Solution of Isopropanol

8.4 Experiment of Analysis of Alcohols by Gas Chromatography

8.5 Online Virtual Experiment of Analysis of Alcohols by Gas Chromatography

Test of Gas Chromatography

Charpter9 Liquid Chromatography Experiment

9.1 Determination of Content of Acetylsalicylic Acid--Principles

9.2 Determination of Content of Acetylsalicylic Acid--Experiment

9.3 Online Virtual Experiment of Determination of Acetylsalicylic Acid

Test of Liquid Chromatography

Charpter10 Comprehensive Experiment

10.1 Principles of Analysis of Nickel Plating Solution

10.2 Experiment of Analysis of Nickel Plating Solution

10.3 Online Virtual Experiment of Analysis of Nickel Plating Solution

Test of Analysis of Nickel Plating Solution

展开全部
预备知识

     In order to better study and master this course, you need

to have the following basic knowledge:


    1. Basic knowledge of middle school chemistry.

    2. Theoretical knowledge of inorganic chemistry.

    3. Theoretical knowledge of analytical chemistry.


Please complete the courses of college physics, inorganic

chemistry, analytical chemistry and general chemistry before studying this

course.

参考资料

1. James Holler and Stanley R. Crouch, Skoog and West’s Fundamentals of Analytical Chemistry (Ninth edition), UK.

2. Daniel C. Harris, Quantitative chemical analysis(Fourth edition) , New York, 1995. 

3. Changgong Meng etc., Experiment for Fundamental Chemistry(Third edition) , China, 2019. 

Dalian University of Technology
5 位授课老师
Yan SU

Yan SU

Professor Senior Engineer, Deputy director of national experimental teaching demonstration center

YongCe Zhang

YongCe Zhang

Engineer

Yuzhen Pan

Yuzhen Pan

Associate Professor, deputy director of the National Experimental Teaching Demonstration Center

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